RT Conference Proceedings T1 Synthesis and characterization of a novel mesoporous silica funtionalized whith [1,5 bis (di-2-pyridyl) methylene thiocarbohydrazide] and its application as enrichment sorbent for determination of antimony by FI-HG-ETAAS A1 Siles-Cordero, María Teresa A1 López-Guerrero, María del Mar A1 Vereda-Alonso, Elisa Isabel A1 García-de-Torres, Amparo A1 Cano-Pavón, José Manuel K1 Antimonio AB Antimony is an element of environmental concern due to its toxicity and biological effects and is therefore considered as a priority pollutant by the US Environmental Protection Agency (EPA). Dissolved antimony is present in seawater at very low concentration levels, typical concentrations of Sb in unpolluted water samples are less than 1 µg L-1. Since the concentration of this element in water is very low, high sensitive analytical techniques are required, The system is based on retention of the analyte onto a micro-column filled with a novel mesoporous silica functionalized with [1,5 bis(di-2-pyridyl) methylene] thiocarbohydrazide placed in the injection valve of the FI manifold.   YR 2014 FD 2014-07-24 LK http://hdl.handle.net/10630/7904 UL http://hdl.handle.net/10630/7904 LA spa NO Universidad de Málaga. Campus de Excelencia Internacional Andalucía Tech DS RIUMA. Repositorio Institucional de la Universidad de Málaga RD 19 ene 2026