RT Conference Proceedings T1 Single and solid solutions metal carboxyphosphonates as precursors for phosphorous-containing electrocatalysts A1 López Vergara, Adrián A1 El-Refaei, S.M. A1 Russo, Patricia A. A1 Vilchez, A A1 Losilla, Enrique R. A1 Porras-Vázquez, José Manuel A1 Olivera-Pastor, Pascual A1 Pinna, N A1 Cabeza-Díaz, Aurelio K1 Química inorgánica AB Co1-xFex-HPAA metal phosphonates were prepared and pyrolyzed under N2 and H2/Ar flows. The result-ing powders were structural and electrochemically characterised by XRD and CV, respectively. The ob-tained materials possess different structures depending on the temperature and pyrolysis atmosphere. Samples pyrolized in N2 at 1000 ºC are monophasic diphosphates, while phosphides form in H2/Ar at 850 ºC. Cyclic voltammetry studies indicate that the Co0.5Fe0.5HPAA sample, pyrolized in H2/Ar, exhibits the best behaviour, but further studies are needed to fully understand the role of graphene oxide and pyrazine. YR 2019 FD 2019-07-19 LK https://hdl.handle.net/10630/18085 UL https://hdl.handle.net/10630/18085 LA eng NO Universidad de Málaga. Campus de Excelencia Internacional Andalucía Tech DS RIUMA. Repositorio Institucional de la Universidad de Málaga RD 22 ene 2026