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Listar por autor "Salcedo, Inés R."
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4D nanoimaging of early age cement hydration.
Shirani, Shiva; Cuesta-García, Ana María; Morales-Cantero, Alejandro; Santacruz-Cruz, María Isabel; Díaz, Ana; Trtik, Pavel; Holler, Mirko; Rack, Alexander; Lukic, Bratislav; Brun, Emmanuel; Salcedo, Inés R.; García-Aranda, Miguel Ángel[et al.] (Springer Nature, 2023-05-08)Despite a century of research, our understanding of cement dissolution and precipitation processes at early ages is very limited. This is due to the lack of methods that can image these processes with enough spatial ... -
Accuracy in Cement Hydration Investigations: Combined X-ray Microtomography and Powder Diffraction Analyses
Salcedo, Inés R.; Cuesta-García, Ana María; Shirani, Shiva; León-Reina, Laura; García-Aranda, Miguel Ángel (MDPI, 2021-11-17)Cement hydration is a very complex set of processes. The evolution of the crystalline phases during hydration can be accurately followed by X-ray powder diffraction data evaluated by the Rietveld method. However, accurate ... -
Accuracy in cement hydration investigations: Combined X-ray microtomography and powder diffraction analyses
Salcedo, Inés R.; Cuesta-García, Ana María; Shirani, Shiva; León-Reina, Laura; García-Aranda, Miguel Ángel (2022-06)Cements are multi-phase materials that can be well understood using a multi-technique approach. Furthermore, the hydration of cement pastes is a very complex set of processes. In this work, we focus on the accuracy of the ... -
Ammonia effects on proton conductivity properties of coordination polymers
Pérez-Colodrero, Rosario Mercedes; Salcedo, Inés R.; Bazaga-García, Montse; Olivera-Pastor, Pascual; Moreno-Real, Laureano; Losilla, Enrique R.; Cabeza-Díaz, Aurelio[et al.] (2016-09-22)Crystalline metal phosphonates are referred to as a type of structurally versatile coordination polymers [1]. Many of them contain guest molecules (H2O, heterocyclics, etc.), acidic sites and, furthermore, their structure ... -
Cementos de arcillas calcinadas y caliza preparados en la Universidad de Málaga
Gómez-de-la-Torre, María de los Ángeles; Santacruz-Cruz, María Isabel; Cuesta-García, Ana María; Bernal, Isabel M.R.; Redondo-Soto, Cinthya; Morales-Cantero, Alejandro; Shirani, Shiva; Pérez-Bravo, Raquel; Franco-Duro, Francisco Ignacio; García-Maté, Marta; Salcedo, Inés R.; León-Reina, Laura; García-Aranda, Miguel Ángel[et al.] (2022)Adjuto documento -
Combined use of laboratory X-ray diffraction and microtomography in early age cement hydration.
Cuesta-García, Ana María; Shirani, Shiva; Gómez-de-la-Torre, María de los Ángeles; Santacruz-Cruz, María Isabel; Morales-Cantero, Alejandro; Koufany, Imane; Redondo-Soto, Cinthya; Salcedo, Inés R.; León-Reina, Laura; García-Aranda, Miguel Ángel[et al.] (2023)In situ laboratory X-ray powder diffraction (LXRPD) is widely used for studying cement hydration at early ages. However, this approach has limitations due to the intrinsic characteristics of the main methodologies (flat ... -
Combined use of X-ray diffraction and microtomography for accurate cement hydration studies.
García-Aranda, Miguel Ángel; Cuesta-García, Ana María; Shirani, Shiva; Gómez-de-la-Torre, María de los Ángeles; Santacruz-Cruz, María Isabel; Morales-Cantero, Alejandro; Koufany, Imane; Redondo-Soto, Cinthya; Salcedo, Inés R.; León-Reina, Laura[et al.] (2023)Ver fichero adjunto que contiene toda la información incluyendo imagenes -
Electrochemical and photochemical applications of multifunctional metal phosphonates
Salcedo, Inés R. (UMA Editorial, 2021-02-09)In this PhD thesis, proton conductivity, photocatalytic and luminescence properties of synthesised multifunctional metal phosphonates have been studied. Iron and zinc derivatives of the R,S hydroxyphosphonoacetic acid ... -
Empleo conjunto de difracción de rayos X de polvo y microtomografía de laboratorio en la hidratación del cemento Portland.
Fernández-Sánchez, Jaime; Cuesta-García, Ana María; Shirani, Shiva; Redondo-Soto, Cinthya; Gómez-de-la-Torre, María de los Ángeles; Santacruz-Cruz, María Isabel; León-Reina, Laura; Salcedo, Inés R.; García-Aranda, Miguel Ángel[et al.] (2023)Se trataron los aspectos más generales sobre la química del cemento, la ciencia del hormigón, el empleo de nuevos materiales más eco-eficientes en la preparación de nuevos sistemas cementantes, revalorización de residuos ... -
From light to heavy alkali metal tetraphosphonates (M = Li, Na, K, Rb, Cs): cation size-induced structural diversity and waterfacilitated proton conductivity
Salcedo, Inés R.; Pérez-Colodrero, Rosario Mercedes; Bazaga-García, Montse; Vasileiou, Antonia; Papadaki, Maria; Olivera-Pastor, Pascual; Infantes-Molina, Antonia; Ramírez-Losilla, Enrique; Mezei, Gellert; Cabeza-Díaz, Aurelio; Demadis, Konstantinos D.[et al.] (The Royal Society of Chemistry, 2018-09)A family of alkali metal-based frameworks containing the tetraphosphonate ligand hexamethylenediamine- N,N,N′,N′-tetrakisIJmethylenephosphonic acid), HDTMP, is reported. A cation size-induced structural diversity, from ... -
High-Throughput Synthesis of Pillared-Layered Magnesium Tetraphosphonate Coordination Polymers: Framework Interconversions and Proton Conductivity Studies
Pérez-Colodrero, Rosario Mercedes; Salcedo, Inés R.; Bazaga-García, Montse; Barouda, Eleni; Papadaki, Maria; Papathanasiou, Konstantinos E.; Hernández Alonso, Daniel; Rius, Jordi; García-Aranda, Miguel Ángel; Ramírez-Losilla, Enrique; Olivera-Pastor, Pascual; Demadis, Konstantinos D.; Cabeza-Díaz, Aurelio[et al.] (MDPI, www.mdpi.com/journal/inorganics, 2018-09-11)Novel pillared-layered framework materials were synthesized by high-throughput or microwave-assisted methodology that contain Mg2+ and the zwitterionic linker HDTMP (hexamethylenediamine-N,N,N0,N0-tetrakis(methylenephosphonic ... -
In situ high pressure powder diffraction study of proton conductors based on metal phosphonates
Bazaga-García, Montse; Pérez-Colodrero, Rosario Mercedes; Olivera-Pastor, Pascual; Losilla, Enrique R.; Salcedo, Inés R.; Wright, Paul A.; García-Aranda, Miguel Ángel; Cabeza-Díaz, Aurelio[et al.] (2015-06-30)Soft Porous Metal Organic frameworks (MOFs) are referred to as a class of coordination polymers that exhibit structural flexibility in response to guest interactions or physical stimuli [1]. By combining softness and ... -
Layered Lanthanide Sulfophosphonates and Their Proton Conduction Properties in Membrane Electrode Assemblies
Bazaga-García, Montse; Salcedo, Inés R.; Pérez-Colodrero, Rosario Mercedes; Xanthopoulos, Konstantinos; Villemin, Didier; Stock, Norbert; López-González, Mar; Del Río, Carmen; Ramírez-Losilla, Enrique; Cabeza-Díaz, Aurelio; Demadis, Konstantinos D.; Olivera-Pastor, Pascual[et al.] (ACS publications, 2019-11-07)Metal phosphonates containing acidic groups exhibit a wide range of proton conduction properties, which may enhance the performance of membrane electrode assemblies (MEAs). In this work, focus is placed on proton conduction ... -
Luminescent and Proton Conducting Lanthanide Coordination Networks Based On a Zwitterionic Tripodal Triphosphonate
Bazaga-García, Montse; Angeli, Giasemi K.; Papathanasiou, Konstantinos E.; Salcedo, Inés R.; Olivera-Pastor, Pascual; Losilla, Enrique R.; Choquesillo-Lazarte, Duane; Hix, Gary B.; Cabeza-Díaz, Aurelio; Demadis, Konstantinos D.[et al.] (American Chemical Society, 2016-07-14)The synthesis, structural characterization, luminescence properties, and proton conduction performance of a new family of isostructural cationic 2D layered compounds are reported. These have the general formula ... -
Mix and measure - Combining in situ X-ray powder diffraction and microtomography for accurate hydrating cement studies.
Shirani, Shiva; Cuesta-García, Ana María; Gómez-de-la-Torre, María de los Ángeles; Santacruz-Cruz, María Isabel; Koufany, Imane; Redondo-Soto, Cinthya; Salcedo, Inés R.; León-Reina, Laura; García-Aranda, Miguel Ángel[et al.] (Elsevier, 2023-11-14)It is reported an innovative methodology based on in situ MoKα1 laboratory X-ray powder diffraction (LXRPD) and microtomography (μCT) avoiding any sample conditioning. The pastes are injected in 2.0 mm capillaries and the ... -
Mix and measure II: joint high-energy laboratory powder diffraction and microtomography for cement hydration studies
Fernández-Sánchez, Jaime; Cuesta, Ana; Shirani, Shiva; Redondo-Soto, Cinthya; Torre, Ángeles G. de la; Santacruz-Cruz, María Isabel; Salcedo, Inés R.; León-Reina, Laura; García-Aranda, Miguel Ángel[et al.] (Wiley, 2024)Portland cements (PCs) and cement blends are multiphase materials of different fineness, and quantitatively analysing their hydration pathways is very chal- lenging. The dissolution (hydration) of the initial crystalline ... -
Mix and measure II: joint high-energy laboratory powder diffraction and microtomography for cement hydration studies
Fernández-Sánchez, Jaime; Cuesta, Ana; Shirani, Shiva; Redondo-Soto, Cinthya; Gómez-de-la-Torre, María de los Ángeles; Santacruz-Cruz, María Isabel; Salcedo, Inés R.; León-Reina, Laura; García-Aranda, Miguel Ángel[et al.] (A. H. Liu, HPSTAR and Harbin Institute of Technology, People's Republic of China, 2024) -
Multimodal study of unaltered cement hydrating pastes: combined high-energy laboratory powder diffraction and microtomography.
Fernández-Sánchez, Jaime; Cuesta, Ana; Shirani, Shiva; Koufany, Imane; Gómez-de-la-Torre, María de los Ángeles; Santacruz-Cruz, María Isabel; Salcedo, Inés R.; León-Reina, Laura; García-Aranda, Miguel Ángel[et al.] (2024)Background: The study of the hydration pathways of Portland cement (PC) and cement blends presents significant challenges due to their multiphase nature and varying fineness. Quantifying the dissolution of initial crystalline ... -
New directions in metal phosphonate and fhosphinate chemistry
Shearan, Stephen J.I.; Stock, Norbert; Emmerling, Franziska; Demel, Jan; Wright, Paul A.; Demadis, Konstantinos D.; Vassaki, Maria; Costantino, Ferdinando; Vivani, Riccardo; Sallard, Sébastien; Salcedo, Inés R.; Cabeza-Díaz, Aurelio; Taddei, Marco[et al.] (MDPI www.mdpi.com/journal/crystals, 2019-05-24)In September 2018, the First EuropeanWorkshop on Metal Phosphonates Chemistry brought together some prominent researchers in the field of metal phosphonates and phosphinates with the aim of discussing past and current ... -
New multifuncional divalent metal-coordinated sulfophosphonates: structures and proton conductivities
Bazaga-García, Montse; Pérez-Colodrero, Rosario Mercedes; Salcedo, Inés R.; Olivera-Pastor, Pascual; Cabeza-Díaz, Aurelio; Demadis, Konstantinos D.[et al.] (2021-01-29)Metal phosphonate-based coordination polymers are structurally versatile multifunctional compounds that may contain a number of acidic groups such as P-OH; SO3H, COOH, N+-H…These features result in formation of extended ...