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Listar por autor "Shirani, Shiva"
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4D Early Age Cement Hydration Analysis by Ptychographic X-ray Computed Tomography and Machine Learning Segmentation
Shirani, Shiva; Cuesta-García, Ana María; Díaz, Ana; García-Aranda, Miguel Ángel; Trtik, Pavel; Holler, Mirko[et al.] (2022-06)Cement manufacturing is responsible for ~7% of the anthropogenic CO2 emissions and hence, decreasing the CO2 footprint, in a sustainable, safe and cost-effective way, is a top priority. To fully understand the binder main ... -
4D nanoimaging of early age cement hydration.
Shirani, Shiva; Cuesta-García, Ana María; Morales-Cantero, Alejandro; Santacruz-Cruz, María Isabel; Díaz, Ana; Trtik, Pavel; Holler, Mirko; Rack, Alexander; Lukic, Bratislav; Brun, Emmanuel; Salcedo, Inés R.; García-Aranda, Miguel Ángel[et al.] (Springer Nature, 2023-05-08)Despite a century of research, our understanding of cement dissolution and precipitation processes at early ages is very limited. This is due to the lack of methods that can image these processes with enough spatial ... -
4D nanoimaging of Portland cement hydration.
Shirani, Shiva; Cuesta, Ana; Díaz, Ana; Trtik, Pavel; Holler, Mirko; Rack, Alexander; Lukic, Bratislav; Brun, Emmanuel; García-Aranda, Miguel Ángel[et al.] (2024)Portland cements are environmentally contentious, accounting for ≈8% of the anthropogenic CO2 emissions. The understanding of the cement hydration reactions (dissolution and precipitation processes) is important to contribute ... -
Accuracy in Cement Hydration Investigations: Combined X-ray Microtomography and Powder Diffraction Analyses
Salcedo, Inés R.; Cuesta-García, Ana María; Shirani, Shiva; León-Reina, Laura; García-Aranda, Miguel Ángel (MDPI, 2021-11-17)Cement hydration is a very complex set of processes. The evolution of the crystalline phases during hydration can be accurately followed by X-ray powder diffraction data evaluated by the Rietveld method. However, accurate ... -
Accuracy in cement hydration investigations: Combined X-ray microtomography and powder diffraction analyses
Salcedo, Inés R.; Cuesta-García, Ana María; Shirani, Shiva; León-Reina, Laura; García-Aranda, Miguel Ángel (2022-06)Cements are multi-phase materials that can be well understood using a multi-technique approach. Furthermore, the hydration of cement pastes is a very complex set of processes. In this work, we focus on the accuracy of the ... -
Advanced 3D nanoimaging of cement paste hydration using synchrotron Xray ptychographic tomography
Shirani, Shiva; Cuesta, Ana; Santacruz-Cruz, María Isabel; Gómez-de-la-Torre, María de los Ángeles; Diaz, Ana; Trtik, Pavel; Holler, Mirko; García-Aranda, Miguel Ángel[et al.] (2024-06-25)Hydration of Portland cements (PC) is a complex phenomenon caused by the presence of multiple components with multi-length scale variability. To investigate this complicated process, state-of-theart 3D nanoimaging ... -
Advanced quantitative synchrotron X-ray imaging of cement micro- and meso- structures
Shirani, Shiva (UMA Editorial, 2023)La tesis se centra en la investigación relacionada con la producción y el comportamiento de varios tipos de cemento, particularmente el cemento Portland y los cementos belíticos, así como los cementos de aluminato cálcico. ... -
ANALYSIS OF BUILDING MATERIALS BY SYNCHROTRON X-RAY IMAGING
Shirani, Shiva; Cuesta-García, Ana María; Morales-Cantero, Alejandro; Gómez-de-la-Torre, María de los Ángeles; Santacruz-Cruz, María Isabel; García-Aranda, Miguel Ángel[et al.] (-, 2021-01)Building materials have complex hierarchical microstructures. The largest components are coarse aggregates with dimensions larger than a few centimetres and the smallest ones are the calcium silicate hydrate (C-S-H) gel ... -
Analysis of cementitious building materials by synchrotron x-ray imaging
Shirani, Shiva (2022)Cement manufacturing especially Portland Cement, the main component for the fabrication of concretes, is the most used building and construction material which has complex hierarchical microstructures. Quantitative ... -
Belite hydration at high temperature and pressure by in situ synchrotron powder diffraction
Morales-Cantero, Alejandro; Gómez-de-la-Torre, María de los Ángeles; Cuesta-García, Ana María; Fraga-López, Edmundo; Shirani, Shiva; García-Aranda, Miguel Ángel[et al.] (2020-10-16)Portland cements are currently used as Oil‐Well‐Cements for the sheath between the metal casing and the borehole. At high pressures and temperatures, the resulting C-S-H gel(s) is partly unstable and it can react to give ... -
Calcium aluminate cement conversion analysed by ptychographic nanotomography
Shirani, Shiva; Cuesta-García, Ana María; Gómez-de-la-Torre, María de los Ángeles; Díaz, Ana; Trtrik, Pavel; Holler, Mirko; García-Aranda, Miguel Ángel[et al.] (Elsevier, 2020-08-17)Calcium aluminate cements are used for special applications but are nowadays banned for general structural purposes due to the calcium aluminate hydrate conversion, that has led, for concretes fabricated with high water ... -
Cementos de arcillas calcinadas y caliza preparados en la Universidad de Málaga
Gómez-de-la-Torre, María de los Ángeles; Santacruz-Cruz, María Isabel; Cuesta-García, Ana María; Bernal, Isabel M.R.; Redondo-Soto, Cinthya; Morales-Cantero, Alejandro; Shirani, Shiva; Pérez-Bravo, Raquel; Franco-Duro, Francisco Ignacio; García-Maté, Marta; Salcedo, Inés R.; León-Reina, Laura; García-Aranda, Miguel Ángel[et al.] (2022)Adjuto documento -
Combined use of laboratory X-ray diffraction and microtomography in early age cement hydration.
Cuesta-García, Ana María; Shirani, Shiva; Gómez-de-la-Torre, María de los Ángeles; Santacruz-Cruz, María Isabel; Morales-Cantero, Alejandro; Koufany, Imane; Redondo-Soto, Cinthya; Salcedo, Inés R.; León-Reina, Laura; García-Aranda, Miguel Ángel[et al.] (2023)In situ laboratory X-ray powder diffraction (LXRPD) is widely used for studying cement hydration at early ages. However, this approach has limitations due to the intrinsic characteristics of the main methodologies (flat ... -
Combined use of X-ray diffraction and microtomography for accurate cement hydration studies.
García-Aranda, Miguel Ángel; Cuesta-García, Ana María; Shirani, Shiva; Gómez-de-la-Torre, María de los Ángeles; Santacruz-Cruz, María Isabel; Morales-Cantero, Alejandro; Koufany, Imane; Redondo-Soto, Cinthya; Salcedo, Inés R.; León-Reina, Laura[et al.] (2023)Ver fichero adjunto que contiene toda la información incluyendo imagenes -
Empleo conjunto de difracción de rayos X de polvo y microtomografía de laboratorio en la hidratación del cemento Portland.
Fernández-Sánchez, Jaime; Cuesta-García, Ana María; Shirani, Shiva; Redondo-Soto, Cinthya; Gómez-de-la-Torre, María de los Ángeles; Santacruz-Cruz, María Isabel; León-Reina, Laura; Salcedo, Inés R.; García-Aranda, Miguel Ángel[et al.] (2023)Se trataron los aspectos más generales sobre la química del cemento, la ciencia del hormigón, el empleo de nuevos materiales más eco-eficientes en la preparación de nuevos sistemas cementantes, revalorización de residuos ... -
Influence of curing temperature on belite cement hydration: a comparative study with Portland cement
Shirani, Shiva; Cuesta-García, Ana María; Morales-Cantero, Alejandro; Gómez-de-la-Torre, María de los Ángeles; Olbinado, Margie P.; García-Aranda, Miguel Ángel[et al.] (Elsevier, 2021-05-24)Belite cements (BCs) could be a more sustainable binder than Portland cements (PCs) but adequate knowledge of the hydration features has still to be built. In particular, the mild curing hydration temperature effects have ... -
Mix and measure - Combining in situ X-ray powder diffraction and microtomography for accurate hydrating cement studies.
Shirani, Shiva; Cuesta-García, Ana María; Gómez-de-la-Torre, María de los Ángeles; Santacruz-Cruz, María Isabel; Koufany, Imane; Redondo-Soto, Cinthya; Salcedo, Inés R.; León-Reina, Laura; García-Aranda, Miguel Ángel[et al.] (Elsevier, 2023-11-14)It is reported an innovative methodology based on in situ MoKα1 laboratory X-ray powder diffraction (LXRPD) and microtomography (μCT) avoiding any sample conditioning. The pastes are injected in 2.0 mm capillaries and the ... -
Mix and measure II: joint high-energy laboratory powder diffraction and microtomography for cement hydration studies
Fernández-Sánchez, Jaime; Cuesta, Ana; Shirani, Shiva; Redondo-Soto, Cinthya; Torre, Ángeles G. de la; Santacruz-Cruz, María Isabel; Salcedo, Inés R.; León-Reina, Laura; García-Aranda, Miguel Ángel[et al.] (Wiley, 2024)Portland cements (PCs) and cement blends are multiphase materials of different fineness, and quantitatively analysing their hydration pathways is very chal- lenging. The dissolution (hydration) of the initial crystalline ... -
Mix and measure II: joint high-energy laboratory powder diffraction and microtomography for cement hydration studies
Fernández-Sánchez, Jaime; Cuesta, Ana; Shirani, Shiva; Redondo-Soto, Cinthya; Gómez-de-la-Torre, María de los Ángeles; Santacruz-Cruz, María Isabel; Salcedo, Inés R.; León-Reina, Laura; García-Aranda, Miguel Ángel[et al.] (A. H. Liu, HPSTAR and Harbin Institute of Technology, People's Republic of China, 2024) -
Multimodal study of unaltered cement hydrating pastes: combined high-energy laboratory powder diffraction and microtomography.
Fernández-Sánchez, Jaime; Cuesta, Ana; Shirani, Shiva; Koufany, Imane; Gómez-de-la-Torre, María de los Ángeles; Santacruz-Cruz, María Isabel; Salcedo, Inés R.; León-Reina, Laura; García-Aranda, Miguel Ángel[et al.] (2024)Background: The study of the hydration pathways of Portland cement (PC) and cement blends presents significant challenges due to their multiphase nature and varying fineness. Quantifying the dissolution of initial crystalline ...