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Advanced synchrotron studies of ye'elimite-based cement pastes
(2018-07-18)
Synchrotron characterization techniques [1] are being used to study Portland-based cements and recently also CSA and related cements. A key property of these techniques is that they do not require sample preparation, so ...
Early hydration study of standard and doped Alite-Belite-Ye’elimite (ABY) cements through Synchrotron Radiation
(2018-07-09)
The manufacturing of ye'elimite-rich cements releases from 15 to 37%, depending on their
composition, less CO2 to the atmosphere than ordinary Portland cement (OPC). BYF cements
containing belite, ye’elimite and ferrite ...
Clinkering of calcium sulfoaluminate clinkers: polymorphism of ye'elimite
(2018)
The manufacture of CSA cements is more environmentally friendly than that of OPC as it releases
less CO2. This reduction depends on CSA composition and is due to three factors: i) less emissions
from decarbonation in the ...
Synchrotron x-ray pair distribution function: A tool to characterize cement gels
(2018-07-06)
Cement matrices contain large amounts of crystalline phases jointly with amorphous and/or nanocrystalline phases. Consequently, their analyses are very challenging. Synchrotron powder diffraction in combination with the ...
Applications of synchrotron x-ray powder diffraction in hydrated cements: high-resolution and high-pressure studies
(2016-07-12)
The main aim of this study is to apply synchrotron radiation techniques for the study of hydrated cement pastes. In particular, the tetracalcium aluminoferrite phase, C4AF in cement nomenclature, is the major iron-containing ...
Aluminum Hydroxide Gel Characterization within a Calcium Aluminate Cement Paste by Combined Pair Distribution Function and Rietveld Analyses
(Elsevier, 2017-06)
There are many commercially important multiphase materials which contain amorphous phases, such as cement
pastes, porcelains, glass-ceramics or pharmaceutical compounds. However, the analysis of amorphous phase(s)
within ...
Amorphous determination in calcium sulfoaluminate materials by external and internal methods
(ICE Publishing, 2014)
External standard methodology has been successfully applied to quantify the known amounts of amorphous component that are increasingly added to cement-related materials. The consistency and accuracy of the methodology were ...
Pair distribution function studies in cementitious systems
(2017-10-24)
The analysis of amorphous/nanocrystalline phase(s) within cement matrices that contain high amounts of crystalline phase(s) is very challenging. Synchrotron techniques can be very useful to characterize such complex samples.1 ...
Ptychographic X-ray computed tomography analysis of cement pastes
(2019-10-04)
Ptychographic X-ray computed tomography provides 3D electron mass density and attenuationcoefficient distributions of unaltered cement pastes with an isotropic resolution below 100 nm. Thisimaging technique allows ...
A comparative study of experimental configurations in synchrotron pair distribution function
(MDPI - Publisher of Open Access Journals, 2019-04-25)
The identification and quantification of amorphous components and nanocrystalline phases
with very small crystal sizes, smaller than ~3 nm, within samples containing crystalline phases is
very challenging. However, this ...