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dc.contributor.authorDe Matos, Paulo R.
dc.contributor.authorNeto, José da Silva Andrade
dc.contributor.authorJansen, Daniel
dc.contributor.authorGómez-de-la-Torre, María de los Ángeles 
dc.contributor.authorKirchheim, Ana Paula
dc.contributor.authorCampos, Carlos E. M.
dc.date.accessioned2022-09-28T10:04:46Z
dc.date.available2022-09-28T10:04:46Z
dc.date.issued2022
dc.identifier.citationCement and Concrete Research, Volume 162, January 2022, 106988es_ES
dc.identifier.urihttps://hdl.handle.net/10630/25133
dc.description.abstractIn-situ X-ray diffraction (XRD) is a powerful tool to assess the hydration of cementitious materials, providing time-resolved quantitative analysis with reasonable accuracy without disturbing sample. However, the lack of guidelines and well-established procedures for data collection and analysis is the limiting factor for spreading this technique. This paper discussed using in-situ laboratory XRD to assess cement hydration. The first part was dedicated to a literature review on the topic. Then, experimental strategies were discussed, and recommendations related to the data analysis routine were drawn; the advantages and limitations of this technique were also discussed. We can conclude that the critical factors for a successful analysis are the choice of an adequate experimental setup with good statistics and low measurement time, the proper consideration of different amorphous contributions in the XRD pattern, and a good data analysis routine. Independent techniques are highly recommended to support the in-situ XRD data.es_ES
dc.description.sponsorshipPID2020-114650RB-I00es_ES
dc.language.isoenges_ES
dc.publisherElsevieres_ES
dc.rightsinfo:eu-repo/semantics/openAccesses_ES
dc.rights.urihttp://creativecommons.org/licenses/by-nc-nd/4.0/*
dc.subjectHormigón - Microscopíaes_ES
dc.subjectRayos X - Difracciónes_ES
dc.subjectCementoes_ES
dc.subject.otherIn-situ XRDes_ES
dc.subject.otherLaboratory XRDes_ES
dc.subject.otherCement hydrationes_ES
dc.subject.otherDifracción de rayos-Xes_ES
dc.titleIn-situ laboratory X-ray diffraction applied to assess cement hydration.es_ES
dc.typeinfo:eu-repo/semantics/articlees_ES
dc.centroFacultad de Cienciases_ES
dc.identifier.doi10.1016/j.cemconres.2022.106988
dc.rights.ccAttribution-NonCommercial-NoDerivatives 4.0 Internacional*
dc.rights.ccAttribution-NonCommercial-NoDerivatives 4.0 Internacional*
dc.type.hasVersioninfo:eu-repo/semantics/submittedVersiones_ES


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